NT4203 Synthesis of Nanomaterials Syllabus:

NT4203 Synthesis of Nanomaterials Syllabus – Anna University PG Syllabus Regulation 2021

OBJECTIVES

 To explore the basic concepts and ideas involved in the synthesis of nanomaterials and to implement different strategies for synthesizing 0, 1D, 2D nanomaterials.
 To explore the role and application of nanomaterials in various fields.

UNIT I MECHANICAL ALLOYING AND MILLING

Introduction to synthesis of nanostructure materials, bottom-up approach and top-down approach– equipment for mechanical alloying, process variables in milling, Mechanism of alloying, Mechanochemical processing – Thermodynamic Aspects, Powder Contamination , Safety Hazards Related to Mechanical Alloying Processes.

UNIT II CHEMICAL APPROACHES

Sol gel method, Solvothermal and hydrothermal routes, precipitation, Spray pyrolysis, Electro spraying and spin coating routes, Self-assembled monolayers (SAMs), Langmuir-Blodgett (LB) films, micro emulsion polymerization- Template based synthesis of nanomaterials- Electrochemical deposition, Electrophoretic deposition.

UNIT III PHYSICAL APPROACHES

Inert gas condensation technique – arc plasma and laser ablation, Vapor deposition and different types of epitaxial growth techniques (CVD,MOCVD, MBE,ALD)- pulsed laser deposition, Sputtering- Magnetron sputtering – Lithography :Photo/UV/EB/FIB techniques, Dip pen nanolithography, Etching process :Dry and Wet etching, micro contact printing.

UNIT IV NANOPOROUS MATERIALS

Zeolites and Mesoporous materials – Synthesis, properties and applications, Role of nanomaterials and nanomembranes in water purification – Carbon nanotubes and graphene – Core shell nanostructures and hybrid nanocomposites.

UNIT V APPLICATION OF NANOMATERIALS

Overview of nanomaterials properties and their applications, nano paints, nano coating, nanomaterials for renewable energy, Nanoelectronics – Nanobots- Biological Applications.

TOTAL :45 PERIODS

COURSE OUTCOMES:

CO1: At the end of the course the student would Gain knowledge on the various process techniques to synthesis nanostructured materials by clear understanding of growth controlling factors of nanomaterial
CO2: The students acquire knowledge about various kind of nanoporous materials
CO3: The course also gives clear knowledge on the application and implementation of nanomaterials to solve the societal problems

REFERENCES:

1. Guozhong Cao, Nanostructures and Nanomaterials: Synthesis, Properties and
2. Applications, Imperial College Press, London 2004.
3. T. Pradeep, Nano: The Essentials Understanding nanoscience and nanotechnology, Tata McGraw Hill Publishing Company Limited NEW DELHI, 2007.
4. A S Edelstein and R C Cammarata, Nanomaterials Synthesis, Properties and Applications, IOP Publishing Ltd 1996.
5. Frank J. Owens and Charles P.Poole, The Physics and Chemistry of Nano Solids, WileyInterscience, 2008