EV4011 Environmental Monitoring Instruments Syllabus:

EV4011 Environmental Monitoring Instruments Syllabus – Anna University PG Syllabus Regulation 2021

OBJECTIVES:

 To educate the students on various instrumental methods of monitoring the quality of air,
water and soil.

UNIT I FUNDAMENTALS

Wet chemistry methods and their limitations-instrumental methods, selection of method- precision
and accuracy, error in measuring signals- quality control & assurance- sample preservation, sample
preparation and analyte isolation.

UNIT II SPECTROSCOPIC METHODS

Principles, techniques and applications of spectrophotometry, fluorimetry, nephelometry and
turbidimetry, Atomic Absorption Spectrometry (Flame, graphite furnace, cold vapour and hydride
generation), Atomic Emission Spectrometry (AES), flame photometry and Inducted Coupled Plasma
(ICP) – TOC Analyzer

UNIT III CHROMATROGRAPHIC METHODS

Principles, techniques and applications of GC, GC-MS, high performance liquid chromatography
(HPLC) and Ion Chromatography (IC)-hyphenated techniques for environmental contaminant (trace
organics) analysis, ICP-MS

UNIT IV ELECTRO AND RADIO ANALYTICAL METHODS

Principles, techniques and applications of conductometry, potentiometry, coulometry, AOX Analyzer.
amperometry, polarography, electro-capillary analysis, Neutron Activation Analysis (NAA), X-ray
Fluorescence (XRF) and X-ray Diffraction (XRD) methods.

UNIT V CONTINUOUS MONITORING INSTRUMENTS

Principles, techniques and applications of NDIR analyzer for CO, chemiluminescent analyzer for
NOx, fluorescent analyzer for SO2- particulates analysis- auto analyzer for water quality using flow
injection analysis. LIMS.

OUTCOMES:

CO1: Able to select appropriate instrumental method for chemical analysis
CO2: Understand spectroscopic methods of analysis of pollutants
CO3: Select correct method for toxic organics estimation using chromatography methods
CO4: Understand electro and nondestructive methods of analysis
CO5: Familiar with online analyzers

REFERENCES:

1. Willard H. Merritt, L. Dean, D.A. and Settle, F.A. ‘Instrumental methods of analysis Edn.
Words Worth, New York, 2004.
2. Paul R. Loconto Trace Environmental Quantitative Analysis: Principles, Techniques, and
Applications, Marcel Dekker; 2nd Edition , 2005,
3. Ewing Instrumental Methods of Chemical Analysis, 5th Edition, McGraw Hill, New York.1985
4. Reeve, R.N., “Introduction to Environmental Analysis”, Analytical Techniques in the Sciences,
John Wiley & Sons, Chichester, UK, 2002.
5. Barcelo, D.(editor), “Environmental analysis. Techniques, Applications and Quality
Assurance”, Elsevier, The Netherlands, 1996